過硫酸銨是工業(yè)上一種重要的化工原料,其方法之一是通過硫酸銨的電解液中結(jié)晶分離獲得。
順酐廠家提醒其具體過程如下:
Ammonium persulfate is an important chemical raw material in industry, and one of its production methods is obtained by crystallization and separation in the electrolyte of ammonium sulfate. The manufacturer of maleic anhydride reminds them that the specific process is as follows:
原料制備:選擇純度較高的硫酸和銨作為原料,按照一定比例混合制備硫酸銨電解液。
Raw material preparation: Select high-purity sulfuric acid and ammonium as raw materials, and mix them in a certain proportion to prepare ammonium sulfate electrolyte.
電解:將硫酸銨電解液放置在電解槽中加熱一定溫度,注入電解質(zhì),通入直流電,使其進(jìn)行電解反應(yīng)。
Electrolysis: Place the ammonium sulfate electrolyte in an electrolytic cell, heat it to a certain temperature, inject an electrolyte, and apply direct current to conduct an electrolytic reaction.
沉淀:在電解反應(yīng)過程中,過硫酸根離子(HSO4-)與銨離子(NH4+)結(jié)合形成過硫酸銨(NH4HSO4),過硫酸銨在酸性環(huán)境下不溶于水,會形成沉淀。
Precipitation: During the electrolysis reaction process, persulfate ions (HSO4-) combine with ammonium ions (NH4+) to form ammonium persulfate (NH4HSO4). Ammonium persulfate is insoluble in water in acidic environments and can form precipitation.
過濾:將電解液和沉淀分離,采用過濾設(shè)備對沉淀進(jìn)行過濾。
Filtration: Separate the electrolyte and sediment, and use high-efficiency filtration equipment to filter the sediment.
洗滌:采用清水對過濾后的沉淀進(jìn)行多次洗滌,以去除其中的雜質(zhì)和硫酸根離子。
Washing: Wash the filtered sediment multiple times with clean water to remove impurities and sulfate ions.
烘干:將洗滌干凈的過硫酸銨沉淀放入烘箱中進(jìn)行烘干,直其水分含量達(dá)到要求為止。
Drying: Place the washed ammonium persulfate precipitate into an oven for drying until its moisture content meets the requirements.
包裝:烘干后的過硫酸銨通過自動包裝機(jī)進(jìn)行快速封裝,以保證其質(zhì)量和純度。
Packaging: The dried ammonium persulfate is quickly packaged using an automatic packaging machine to ensure its quality and purity.
以上就是工業(yè)中過硫酸銨從硫酸銨的電解液中結(jié)晶分離的主要過程,此外在使用過硫酸銨前,一定要學(xué)習(xí)其性質(zhì)、操作規(guī)程和注意事項。必須穿戴好防護(hù)服、手套和護(hù)目鏡等個人防護(hù)裝備,并在通風(fēng)良好的地方進(jìn)行操作。
The above is the main process of crystallization and separation of ammonium persulfate from ammonium sulfate electrolyte in industrial production. In addition, before using ammonium persulfate, it is necessary to learn its properties, operating procedures, and safety precautions. Wear protective clothing, gloves, goggles and other personal protective equipment, and operate in a well ventilated place.
過硫酸銨應(yīng)該存放在干燥、通風(fēng)、遠(yuǎn)離火源和易燃物品的地方。不要與還原劑、易燃物品和酸性物質(zhì)混放,避免發(fā)生劇烈反應(yīng)。
Ammonium persulfate should be stored in a dry, ventilated place away from ignition sources and flammable materials. Do not mix with reducing agents, flammable substances, and acidic substances to avoid violent reactions.
使用過的過硫酸銨和廢棄物必須正確處理,不可隨意傾倒到下水道或垃圾桶中,應(yīng)該根據(jù)當(dāng)?shù)氐姆ㄒ?guī)和規(guī)定進(jìn)行處理。
The used ammonium persulfate and waste must be properly disposed of and cannot be casually dumped into the sewer or garbage bin. They should be disposed of in accordance with local regulations and rules.
如果不慎發(fā)生濺潑、泄漏或者吸入過量的過硫酸銨,應(yīng)該立即停止工作,迅速脫離現(xiàn)場并取得醫(yī)療支持。同時,應(yīng)該按照事故應(yīng)急預(yù)案采取緊急措施,使人員和環(huán)境得到保護(hù)。針對此產(chǎn)品設(shè)備的事項,還有什么不了解的或者有什么需求,都可以隨時來咨詢聯(lián)系我們
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If splashing, leakage, or inhalation of excessive ammonium persulfate occurs accidentally, work should be stopped immediately, and medical support should be obtained by quickly leaving the scene. At the same time, emergency measures should be taken in accordance with the accident emergency plan to protect personnel and the environment. If you have any questions or needs regarding the equipment of this product, please feel free to contact us at any time http://qugjs.com.cn !